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Complexes of esters of ethylenediphosphonic acid with lanthanide nitrates—synthesis and structure

✍ Scribed by Erhard T. K. Haupt; Jürgen Kopf; Jordanka Petrova; Vladislav Arabadzhiev; Snezhana Momchilova

Publisher
John Wiley and Sons
Year
2006
Tongue
English
Weight
219 KB
Volume
17
Category
Article
ISSN
1042-7163

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✦ Synopsis

The lanthanide complexes L 2 Ln(NO 3 ) 3

(3) and L 3 [Ln(NO 3 ) 3 ] 2 (5) (Stewart and Siddall III.

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Complexes of diethyl-2-amino-2-oxoethylp
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## Abstract Lanthanide complexes LnL~2~(NO~3~)~3~ **3a–f** are obtained where Ln is La, Ce, Sm, Eu, Er, and Yb and L is the diethyl 2‐amino‐2‐oxoethylphosphonate. They were characterized by elemental analysis, IR, and NMR spectroscopy. Monodentate coordination by the phosphoryl group is suggested f

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The lanthanide nitrate complexes with 13-crown-4(13-C-4) have been prepared in AcOEt. These new complexes with the general formula Ln(N03),.(13-C-4) (Ln = La-Nd, Sm-Lu) have been characterized by means of elemental analysis, IR and 'H-NMR spectra, conductivity measurements, and TG-DTA techniques. Th