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Complexes of 2,4,4,5,5-pentamethyl-1-pyrroline and 2,4,4,5,5-pentamethyl-1-pyrroline 1-oxide: Preparation and properties of tetrahedral Co(II) complexes

✍ Scribed by James D. Navratil; Steven S. Zumdahl

Book ID: 115973271
Publisher: Elsevier Science
Year: 1974
Weight: 571 KB
Volume: 36
Category: Article
ISSN: 0022-1902
DOI: 10.1016/0022-1902(74)80254-x

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## Abstract The title compound **1** is shown to give, both upon direct irradiation at 254 nm and upon acetophenone‐sensitized photolysis at 300 nm, the __syn__‐vinyl‐pentamethylhousene **5**, which spontaneously rearranges in a [3,3]0sigmatropic process to give the bicyclo[3.2.0]heptadiene skeleto