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Complexation of tin(II) chloride by a novel macrocycle containing rhodium and nitrogen binding sites. The preparation and x-ray crystal structure of Rh2Sn2(CO)2Cl6[.mu.-2,6-bis(diphenylphosphino)pyridine]2

✍ Scribed by Balch, Alan L.; Hope, Hakon; Wood, Fred E.

Book ID: 120475320
Publisher: American Chemical Society
Year: 1985
Tongue: English
Weight: 734 KB
Volume: 107
Category: Article
ISSN: 0002-7863
DOI: 10.1021/ja00310a032

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## Abstract The complex __trans__‐[RuCl~2~{κ^2^‐__P__,__P__‐(__S__)‐peap}~2~] (1) has been stereoselectively prepared by the treatment of a stoichiometric mixture of complex [RuCl~2~(DMSO)~4~] (DMSO = dimethyl sulfoxide) and (__S__)‐peap [(__S__)‐peap = (−)‐__N__,__N__‐bis(diphenylphosphanyl)‐(__S_