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Complete assignments of 1H and 13C NMR spectra of leucanthoside A, a new triterpenoid saponin from Cephalaria leucantha L.

✍ Scribed by D. Gođevac; B. Mandić; V. Vajs; N. Menković; S. Macura; S. Milosavljević

Publisher
John Wiley and Sons
Year
2006
Tongue
English
Weight
213 KB
Volume
44
Category
Article
ISSN
0749-1581

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✦ Synopsis

Abstract

Leucanthoside A, a new allose‐containing triterpenoid saponin (1), was isolated from the aerial parts of Cephalaria leucantha L. Its structure was determined by electrospray ionization mass spectrometry and NMR spectroscopy. Complete assignments of the ^1^H and ^13^C NMR chemical shifts were achieved by two‐dimensional NMR experiments: DQF‐COSY, NOESY, TOCSY, HSQC, DINE‐HSQC, HMBC, ^13^C‐^1^H 2D‐J‐resolved spectroscopy, and 1,1‐ADEQUATE. Copyright © 2006 John Wiley & Sons, Ltd.

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