## Abstract Two novel unsaturated E‐ring pentacyclic triterpenoid saponins, ilexhainanoside A and ilexhainanoside B, were isolated from the leaves of __Ilex hainanensis__. Their chemical structures were determined by MS, NMR spectroscopy and chemical analysis. Complete assignments of the ^1^H and ^
Complete assignments of 1H and 13C NMR data for two new sesquiterpenes from Cyperus rotundus L.
✍ Scribed by Yan Xu; Hong-Wu Zhang; Xiao-Chun Wan; Zhong-Mei Zou
- Publisher
- John Wiley and Sons
- Year
- 2009
- Tongue
- English
- Weight
- 224 KB
- Volume
- 47
- Category
- Article
- ISSN
- 0749-1581
- DOI
- 10.1002/mrc.2416
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✦ Synopsis
Abstract
Two new sesquiterpenes, epi‐guaidiol A (1) and sugebiol (3), together with four known sesquiterpenes, guaidiol A(2), sugetriol triacetate (4), cyperenoic acid (5), and cyperotundone (6) were isolated from the rhizomes of Cyperus rotundus L. Their structures were identified by MS and NMR experiments, and the complete assignments of ^1^H and ^13^C NMR data for two new sesquiterpenes were obtained by the aid of two‐dimensional (2D) NMR techniques, including HSQC, HMBC, ^1^H‐^1^HCOSY and nuclear overhauser enhancement spectroscopy(NOESY). Copyright © 2009 John Wiley & Sons, Ltd.
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