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Complete Assignment of Heteronuclear Protein Resonances by Protonless NMR Spectroscopy

โœ Scribed by Wolfgang Bermel; Ivano Bertini; Luminita Duma; Isabella C. Felli; Lyndon Emsley; Roberta Pierattelli; Paul R. Vasos

Publisher
John Wiley and Sons
Year
2005
Tongue
English
Weight
392 KB
Volume
44
Category
Article
ISSN
0044-8249

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The method of two-dimensional heteronuclear relayed correlation spectroscopy was used to establish the assignment of the severely overcrowded part of the proton spectrum of menthol by relating it to the previously assigned carbon spectrum. Extrapolation of the signal-to-noise ratio obtained with ove