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Complete 1H and 13C NMR assignment of ent-3β,16α-atisanediol, a cytotoxic diterpene isolated from the sponge Spirastrella cunctatrix

✍ Scribed by Francesco Cafieri; Ernesto Fattorusso; Yosef Mahajnah; Alfonso Mangoni


Publisher
John Wiley and Sons
Year
1995
Tongue
English
Weight
392 KB
Volume
33
Category
Article
ISSN
0749-1581

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✦ Synopsis


Full assignment of the 'H and 13C NMR spectra of ent-atisane-3fl,16adiol, a cytotoxic diterpene isolated from the Caribbean sponge Spirustrellu cunctatrix, was achieved by extensive use of two-dimensional NMR spectroscopy and spectral simulation. This is the first complete NMR characterization af an atisane terpene.


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