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Complete 1H and 13C NMR Analysis of an Asymmetric Tröger's Base

✍ Scribed by Carmen Pardo; Mar Ramos; Alain Fruchier; José Elguero

Publisher
John Wiley and Sons
Year
1996
Tongue
English
Weight
243 KB
Volume
34
Category
Article
ISSN
0749-1581

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✦ Synopsis

The 'H and I3C NMR spectra of an asymmetric Troger's base were recorded and the corresponding signals assigned on the basis of long-range coupling constants and 'H-13C correlations. In 1H NMR, ambiguities in the assignment of e m and endo hydrogen atoms and in the long-range couplings between the metbylene hydrogens were resolved.

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