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Comparison of Two Methods of Methyl Group Grafting to the Silica Thin Film Surface and Its Tribological Properties Measured by Atomic Force Microscopy

✍ Scribed by J.P. Grobelny; G. Celichowski; M. Cichomski; A.J. Kulik; I.J. Piwoński; S. Plaza

Book ID
111613897
Publisher
Springer US
Year
2004
Tongue
English
Weight
147 KB
Volume
16
Category
Article
ISSN
1023-8883

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Oxygen interaction of CdS-based gas sens
Oxygen interaction of CdS-based gas sensors with different stoichiometric compositions was studied by X-ray photoelectron spectroscopy (XPS) and thermal-desorption mass spectroscopy observations combined with conductivity measurements. Three different types of film with different atomic ratios of Cd/S were used in the study of oxygen chemisorption in a low-temperature range between 300 and 570 K. Spray pyrolysis was used for the deposition of the films on glass substrates; XPS and energy dispersive spectroscopy of X-ray together with atomic force microscopy and scanning electron microscopy were used for the characterization of the composition and structure of the films. It was possible to distinguish different temperature ranges for the thermal desorption of the different adsorbed oxygen species. A comparison of the data from XPS and mass-spectroscopy observations with conductance measurements allows to conclude that metallic surface atoms are responsible for different interactions of oxygen species with CdS surfaces.
📂 Article 📅 1995 🏛 Elsevier Science 🌐 English ⚖ 379 KB