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Comparison of structure in solid state of new 1,5-bis(4-cyano-2,6-dimethoxyphenoxy)alkanes by means of 13C CP/MAS NMR and X-ray diffraction

✍ Scribed by Jerzy Żabiński; Irena Wolska; Dorota Maciejewska


Publisher
Elsevier Science
Year
2007
Tongue
English
Weight
553 KB
Volume
833
Category
Article
ISSN
0022-2860

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Solid state structure by X-ray and 13C C
✍ Magdalena Rasztawicka; Irena Wolska; Dorota Maciejewska 📂 Article 📅 2007 🏛 Elsevier Science 🌐 English ⚖ 260 KB

5,5 0 -Diethoxy-3,3 0 -methanediyl-bis-indole 1 was synthesized by novel protocol and its solid state structure was analyzed using X-ray diffraction and 13 C CP/MAS NMR methods. Double resonances were observed in the spectrum of 1, and different structure of both indole systems in one molecule (show