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Comparison of four pulse sequences for the routine application of proton-carbon shift correlation

✍ Scribed by H. Kessler; C. Griesinger; G. Zimmermann


Publisher
John Wiley and Sons
Year
1987
Tongue
English
Weight
438 KB
Volume
25
Category
Article
ISSN
0749-1581

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✦ Synopsis


Four different pulse sequences for proton-carbon shift correlation via 'J(CH) couplings are compared using amacrolide as a practical example. These are the COLOC sequence, a new improved variant of COLOC, the 2D-DEPT-COSY sequence and its new constant-time variant. It emerged that the 2D-DEPT-COSY and the modified COLOC sequences are the most appropriate for the purpose of routine proton-carbon shift correlation via direct coupling.