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Comparison between collision induced dissociation of electrosprayed protonated peptides in the up-front source region and in a low-energy collision cell

✍ Scribed by W. D. van Dongen; J. I. T. van Wijk; B. N. Green; W. Heerma; J. Haverkamp


Publisher
John Wiley and Sons
Year
1999
Tongue
English
Weight
66 KB
Volume
13
Category
Article
ISSN
0951-4198

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✦ Synopsis


A systematic comparison between the up-front Collision induced dissociation (CID) mass spectra and low-energy CID tandem mass spectra from twenty-one singly and/or doubly charged peptides has been made. CID spectra of the peptides were recorded at different electrode voltages in the up-front source region of a single quadrupole instrument and different collision energies in the collision cell of a tandem quadrupole instrument. It was observed that up-front CID and low-energy CID yielded comparable product ion spectra from protonated peptides, and that the instrumental settings necessary for obtaining comparable CID mass spectra from the two methods are correlated.