Comparative utility of the silyl ether and acetate ester derivatives of ethinyl estradiol for its quantitative gas chromato-graphic determination

Mixed silyl ether–perfluoroacyl ester de

Mixed silyl ether–perfluoroacyl ester derivatives for gas chromatography/mass spectrometry of oestrogens. Application to the quantitative determination of oestriol in human plasma

✍ L. Dehennin 📂 Article 📅 1989 🏛 John Wiley and Sons 🌐 English ⚖ 480 KB 👁 2 views

The conversion of oestrogens into mixed derivatives comprising a phenolic silyl ether and one or more alcoholic perfluoroactyl ester(s) is described. They are easily formed in quantitative yield and have excellent gas chromate graphic and mass spectrometric properties, making them suitable for analy