## Thin-Layer Chromatographic Separation and Analysis of @'-Labeled Compounds1 The isotopic analysis of oxygen in organic compounds requires the use of fairly large samples for conversion by various methods (1,2) to carbon
Combustion and nonaqueous titration determination of carbon in plant tissues
โ Scribed by Hsu-Ho Chung; M.J. Trlica
- Publisher
- Elsevier Science
- Year
- 1978
- Tongue
- English
- Weight
- 273 KB
- Volume
- 88
- Category
- Article
- ISSN
- 0003-2697
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โฆ Synopsis
A method for determination of total carbon and carbon-14 in biological samples by combustion and subsequent absorption and titration of carbon dioxide in organic amine is described. Results obtained with this method are comparable to those obtained with a carbon analyzer. Fifteen carbon-content determinations and sample preparations for carbon-14 liquid scintillation counting can be performed in 1 hr using this procedure.
Methods
A model 306 Tri-Carb sample oxidizer (Packard Instrument Co.) was used to combust plant samples. A 14C-labeled sample of finely ground freeze-dried plant tissue (ca. 30 mg) was weighed into a microchemical
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