Colorimetric determination of formaldehyde via free radical formation
β Scribed by James W. Munson; Thomas G. Hodgkins
- Publisher
- John Wiley and Sons
- Year
- 1975
- Tongue
- English
- Weight
- 311 KB
- Volume
- 64
- Category
- Article
- ISSN
- 0022-3549
No coin nor oath required. For personal study only.
β¦ Synopsis
Aliphatic aldehydes react with 2,3-dimethyl-2,3-bis-(hydroxylamino)butane and sodium periodate for form colored free radicals. These radicals were stabilized with pyridine in aqueous solution. Low levels of formaldehyde in aqueous solutions were determined utilizing this reaction.
π SIMILAR VOLUMES
Free formaldehyde in nail preparations, extracted with dichloromethane and 0.002 M hydrochloric acid (1:2 v./v.), was determined by differential pulse voltammetry(DPV) using a thin-film mercury electrode (TFME) in a basic solution. The various factors such as deposition time, concentration of mercur
thyldecatriene. With divinylbenzene, both vinyl groups can take part in the reaction, and the products include FH3 FH3 CH=CH-CHZ-C=CH-CH~-CH~-C=CH-CH~ -0 (13) didecatrienylbenzene and vinyldecatrienylbenzene. a-Substituted styrenes such as cr-methylstyrene are much less reactive than styrene itself