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Closo boron hydrides with 13 to 24 boron atoms

โœ Scribed by Brown, Leo D.; Lipscomb, William N.

Book ID
126826388
Publisher
American Chemical Society
Year
1977
Tongue
English
Weight
967 KB
Volume
16
Category
Article
ISSN
0020-1669

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The diethynyldicarba-closo-dodecaboranes 1,2-R 2 -9,12-(HCC) 2 -closo-1,2-C 2 B 10 H 8 [R = H (1a), Me (2a)] and 9,10-(HCC) 2 -closo-1,7-C 2 B 10 H 10 (3a) were obtained by Pd-catalyzed Kumada-type cross-coupling reactions of the corresponding diiodinated dicarba-closo-dodecaboranes with Me 3 SiCCMg