✦ LIBER ✦
cis-Bis[diphenyl(phenylsulfanylmethyl)diphenylphosphine-κP]bis(pentafluorophenyl)gold(III) perchlorate chloroform solvate
✍ Scribed by Jones, Peter G. ;Fernández, Eduardo J. ;López-de-Luzuriaga, José M. ;Laguna, Antonio
- Publisher
- International Union of Crystallography
- Year
- 2006
- Tongue
- English
- Weight
- 138 KB
- Volume
- 62
- Category
- Article
- ISSN
- 1600-5368
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✦ Synopsis
H atoms were included using a riding model with fixed C-H bond lengths of 0.95 (phenyl), 0.99 (methylene), 1.00 A ˚(CHCl 3 ); U iso (H) values were fixed at 1.2 times U eq of the parent atom. To improve refinement stability, a total of 562 restraints were applied to C atom displacement parameters (similarity and rigid-bond restraints) and local ring symmetry (planarity and similarity of distances). The Flack metal-organic papers m1998 Jones et al. [Au(C 6 F 5 ) 2 (C 19 H 17 PS) 2 ]ClO 4 ÁCHCl 3