## Abstract An ion chromatographic procedure (IC) with chemical suppression is described for the simultaneous determination of the anions Cl^โ^, NO, HPO and SO at ppm levels in vinegar samples. The moderately strong eluent composed of NaHCO~3~/Na~2~CO~3~ was chosen and sample pretreatment was requi
Chromatographic Determination of the Phosphate Anions in Crystalline and Glassy Na4NbP3Oz
โ Scribed by B.C. Sales; B.C. Chakoumakos
- Publisher
- Elsevier Science
- Year
- 1993
- Tongue
- English
- Weight
- 127 KB
- Volume
- 105
- Category
- Article
- ISSN
- 0022-4596
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โฆ Synopsis
High-performance liquid chronatography (HPLC) measurements on crystalline and glassy (\mathrm{Na}{4} \mathrm{NbP}{3} \mathrm{O}{2}) prove that the crystalline phase is a pyrophosphate and that the glassy material contains a distribution of phosphate anions with anions up to five (\mathrm{PO}{4}) tetrahedra in length. Powder (\mathrm{X})-ray diffraction data for a new trimetaphosphate crystalline phase with the composition (\mathrm{Na}{3} \mathrm{NbP}{3} \mathrm{O}_{x}) are also reported. O 1993 Academic Press, Inc.
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