A peroxyoxalate chemiluminescence detection in high-performance liquid chromatography was examined for determination of long chain aliphatic aldehydes using 4-(N~-dimethylaminosulphonyl)-7-hydrazino-2,~,3benzoxadiazole (DBD-H) as a fluorogenic labelling reagent. A mixture of 0.6 m M bi~(2,4,6-trichl
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Chromatographic determination of low-molecular mass unsaturated aliphatic aldehydes with peroxyoxalate chemiluminescence detection after fluorescence labeling with 4-(N,N-dimethylaminosulfonyl)-7-hydrazino-2,1,3-benzoxadiazole
โ Scribed by Ali, Marwa Fathy Bakr; Kishikawa, Naoya; Ohyama, Kaname; Mohamed, Horria Abdel-Mageed; Abdel-Wadood, Hanaa Mohamed; Mahmoud, Ashraf Mohamed; Imazato, Takahiro; Ueki, Yukitaka; Wada, Mitsuhiro; Kuroda, Naotaka
- Book ID
- 121819521
- Publisher
- Elsevier Science
- Year
- 2014
- Tongue
- English
- Weight
- 786 KB
- Volume
- 953-954
- Category
- Article
- ISSN
- 1873-376X
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The utility of the fluorescence derivatixation reagents, 4-(N,N-dimethylaminosulfonyl)-7-(2-chloroformylpyrrolidin-l-yl)\_2,1,3-benzoxadiaxole [ R( + J-DBD-Pro-CCC1 and S( -)-DBD-Pro-CCC11 with compounds having various functional groups has been evaluated. Enantiomers of DBD-Pro-COCI were equally re