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Chloro­[2-(1-ethyl-1H-benzimidazol-2-yl)­phenol-κN3][2-(1-ethyl-1H-benzimidazol-2-yl)­phenolato-κ2N3,O]­zinc(II)

✍ Scribed by Tong, Yi-Ping ;Ye, Bao-Hui

Publisher
International Union of Crystallography
Year
2004
Tongue
English
Weight
230 KB
Volume
60
Category
Article
ISSN
1600-5368

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Single-crystal X-ray study T = 297 K Mean '(C±C) = 0.009 A Ê Disorder in main residue R factor = 0.059 wR factor = 0.169 Data-to-parameter ratio = 13.9 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

Bis[2-(1H-benzimidazol-2-yl-κN3)-4,6-dib
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✍ Wu, Yu ;Xie, Bin ;Zou, Like ;Feng, Jian-Shen ;Hu, Zongqiu 📂 Article 📅 2007 🏛 International Union of Crystallography 🌐 English ⚖ 613 KB

The title compound, [Ni(C 13 H 7 Br 2 N 2 O) 2 ], an Ni II complex of the Schiff base 2-(3,5-dibromo-2-hydroxyphenyl)benzimidazole, was synthesized by the reaction of 3,5-dibromosalicylaldehyde and 1,2-phenylenediamine. The molecule resides on a twofold rotation axis. The Ni II atom exists in a dist