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Chlorination of maltose with triphenylphosphine-N-chlorosuccinimide (TPP-NCS) reagent

โœ Scribed by Stanley Z. Dziedzic; Elner B. Rathbone; G.G. Birch

Book ID
103709207
Publisher
Elsevier Science
Year
1984
Tongue
English
Weight
233 KB
Volume
15
Category
Article
ISSN
0308-8146

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Regioselective chlorination of chitin wi
Regioselective chlorination of chitin with N- chlorosuccinimide-triphenylphosphine under homogeneous conditions in lithium chloride-N,N-dimethylacetamide
โœ Munenori Sakamoto; How Tseng; Ken-ichi Furuhata ๐Ÿ“‚ Article ๐Ÿ“… 1994 ๐Ÿ› Elsevier Science ๐ŸŒ English โš– 781 KB

Purified chitin was chlorinated with an equimolar mixture of N-chlorosuccinimide and triphenylphosphine under homogeneous conditions in a 5% (w/v) solution of LiCl in N,N-dimethylacetamide at 70-85"C. 13C NMR spectroscopy of the chlorinated products and gas chromatographic-mass spectrometric analysi