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Chlorination of alkyl glyoxylate phenylhydrazones and triketone phenylhydrazones

✍ Scribed by Moon, M. W.


Book ID
126258540
Publisher
American Chemical Society
Year
1972
Tongue
English
Weight
766 KB
Volume
37
Category
Article
ISSN
0022-3263

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residue remaining on evaporation was chromatographed on 850 g of silica gel (column 4x90 cm) with hexane/acetone (100: 3). The first 300 ml of eluate contained 10.9 g of crude product (30). This was taken up in ether, and washed with 1 % hydrochloric acid and 1 % sodium hydrogen carbonate solution;