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Chiral Amine Synthesis (Methods, Developments and Applications) || Reduction of Imines with Trichlorosilane Catalyzed by Chiral Lewis Bases

✍ Scribed by Nugent, Thomas C.

Publisher: Wiley-VCH Verlag GmbH & Co. KGaA
Year: 2010
Tongue: German
Weight: 268 KB
Edition: 1
Category: Article
ISBN: 3527325093
DOI: 10.1002/9783527629541.ch4

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✦ Synopsis

Edited By Thomas C. Nugent ; [with A Foreword By John Hartwig]. Includes Bibliographical References And Index.

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## Abstract In the aza‐Morita–BaylisHillman reaction of __N__‐sulfonated imines (__N__‐arylmethylidene‐4‐methylbenzenesulfonamides and others) with methyl vinyl ketone (MVK), we found that in the presence of a catalytic amount of the chiral phosphine Lewis bases (__R__)‐(−)‐6,6′‐bis[tris(3,3,4,4,5