Chemoselective Thioacetalization in Water: 3-(1,3-Dithian-2-ylidene)pentane-2,4-dione as an Odorless, Efficient, and Practical Thioacetalization Reagent.
โ Scribed by Dewen Dong; Yan Ouyang; Haifeng Yu; Qun Liu; Jun Liu; Mang Wang; Jing Zhu
- Publisher
- John Wiley and Sons
- Year
- 2005
- Weight
- 20 KB
- Volume
- 36
- Category
- Article
- ISSN
- 0931-7597
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## Abstract ฮฑโOxo ketene dithioacetals, methyl 2โ(1,3โdithian/dithiolanโ2โylidene)โ3โoxobutanoate (**2a/2b**) prepared in nearly quantitative yields simply from methyl acetylacetate, carbon disulfide and 1,3โdibromopropane/1,2โdibroโ moethane in the presence of potassium carbonate, were investigate
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