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Chemoselective conversion of azides to t-butyl carbamates and amines

✍ Scribed by Yeon Joo Jung; Yu Mi Chang; Ji Hee Lee; Cheol Min Yoon

Book ID
104252301
Publisher
Elsevier Science
Year
2002
Tongue
French
Weight
212 KB
Volume
43
Category
Article
ISSN
0040-4039

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✦ Synopsis

Azides were converted to the corresponding carbamates using a system of 20 mol% of decaborane (B 10 H 14 ) and 20 weight% of 10% Pd/C in methanol in the presence of di-tert-butyl dicarbonate at rt in high yields and to the corresponding amines using a system of 10 mol% of decaborane and 20 weight% of 10% Pd/C in methanol in the absence of di-tert-butyl dicarbonate at rt in high yields.

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