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Chemoenzymatic one-pot synthesis of cefazolin from cephalosporin C in fully aqueous medium, involving three consecutive biotransformations catalyzed by D-aminoacid oxidase, glutaryl acylase and penicillin G acylase

✍ Scribed by Roberto Fernández-Lafuente; JoséM. Guisán; Massimo Pregnolato; Marco Terreni


Publisher
Elsevier Science
Year
1997
Tongue
French
Weight
190 KB
Volume
38
Category
Article
ISSN
0040-4039

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✦ Synopsis


A new chemoenzymatic synthesis of Cefazolin through the correct assembly of three bioU'ansformations catalysed by D-aminoacid oxidase, glutaryl acylase and penicillin G acylase is described. This multienzymatic synthesis has been performed from the natural Cephalosporin C in fully aqueous medium without intermediate purification stages. Almost quantitative yields have been achieved in all the enzymatic reactions.