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ChemInform Abstract: α-Thioxothioamides: [4 + 2] and [2 + 2] Cycloaddition Reactions with Aryl Isothiocyanates and Phenyl Isocyanate.

✍ Scribed by E. MARCHAND; G. MOREL

Publisher
John Wiley and Sons
Year
2010
Weight
43 KB
Volume
29
Category
Article
ISSN
0931-7597

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1,3-Thiazepines. Part 2. Reaction of 2-Iminohexahydrothiazepines with Phenyl Isocyanate and Isothiocyanates. -Reaction of the iminothiazepines (I) with phenyl isocyanate (II) gives the expected ureas (III) in good yields. In contrast, reaction with aryl isothiocyanates in refluxing toluene produces