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ChemInform Abstract: ZnVSe2O7 and Cd6V2Se5O21: New d10 Transition-Metal Selenites with V(IV) or V(V) Cations.

✍ Scribed by Hai-Long Jiang; Fang Kong; Yang Fan; Jiang-Gao Mao

Publisher: John Wiley and Sons
Year: 2008
Weight: 27 KB
Volume: 39
Category: Article
ISSN: 0931-7597
DOI: 10.1002/chin.200846019

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Crystal Structures of 3.0.CO;2-Z/asset/equation/tex2gif-stack-1.gif?v=1&t=h5l6migq&s=c6023d23614cc5febe987fafc1b321310df66e88" class="inlineGraphic">{[Cd(phen)](C6H8O4)3/3} and 3.0.CO;2-Z/asset/equation/tex2gif-stack-2.gif?v=1&t=h5l6migr&s=ca7048152611c2fb5494587a82e9d48966405110" class="inlineGraphic">{[Cd(phen)](C7H10O4)3/3} · 2H2O with C6H10O4 = Adipic Acid and C7H12O4 = Pimelic Acid

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Two coordination polymers 1 ϱ {[Cd(phen)](C 6 H 8 O 4 ) 3/3 } (1) and 1 ϱ {[Cd(phen)](C 7 H 10 O 4 ) 3/3 } • 2H 2 O (2) were structurally characterized by single crystal X-ray diffraction methods. In 1 (C2/ c (no. 15), a ϭ 16.169(2) A ˚, b ϭ 15.485(2) A ˚, c ϭ 14.044(2) A ˚, β ϭ 112.701(8)°, U ϭ 324

Rapid and Simple Isolation of the Crysta

Rapid and Simple Isolation of the Crystalline Molybdenum-Blue Compounds with Discrete and Linked Nanosized Ring-Shaped Anions: Na15[Mo3.0.CO;2-%23/asset/equation/tex2gif-stack-1.gif?v=1&t=h5l566t6&s=c0a09f77518ccacb50e822358608409f8e1c0a41" class="inlineGraphic">Mo3.0.CO;2-%23/asset/equation/tex2gif-stack-2.gif?v=1&t=h5l566t6&s=3b4dd445e7e4356504ec58daf107b378c9736f7b" class="inlineGraphic">O462H14(H2O)70]0.5 [Mo3.0.CO;2-%23/asset/equation/tex2gif-stack-3.gif?v=1&t=h5l566t6&s=32c4cd6315aa03537e50d3683e9830279c928f78" class="inlineGraphic">Mo3.0.CO;2-%23/asset/equation/tex2gif-stack-4.gif?v=1&t=h5l566t7&s=3a1388422ef00ab21b32f2e8ba73a564490bf0c1" class="inlineGraphic">O457H14(H2O)68]0.5 · ca. 400 H2O and Na22[Mo3.0.CO;2-%23/asset/equation/tex2gif-stack-5.gif?v=1&t=h5l566t7&s=2f041805f3359c66af741d31ef3916871c113c35" class="inlineGraphic">Mo3.0.CO;2-%23/asset/equation/tex2gif-stack-6.gif?v=1&t=h5l566t7&s=e3f6eced1d8e1eea086310b68afe457fcdf2951e" class="inlineGraphic">O442H14(H2O)58] · ca. 250 H2O

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The blue mixed-crystal title compound Na 15 [Mo VI 126 Mo V 28 O 462 H 14 (H 2 O) 70 ] 0.5 [Mo VI 124 Mo V 28 O 457 H 14 (H 2 O) 68 ] 0.5 ´ca. 400 H 2 O º Na 15 [1 a] 0.5 [1 b] 0.5 ´ca. 400 H 2 O 1, which crystallizes in the triclinic space group P 1 (a = 30.785(2), b = 32.958(2), c = 47.318(3) A Ê