ChemInform Abstract: trans-1,3-Diethoxy-5,5-dimethyl-1,3-diphospha-5-silacyclohexane-1,3-dion e.
β Scribed by P. G. JONES; A. WEINKAUF
- Publisher
- John Wiley and Sons
- Year
- 2010
- Weight
- 24 KB
- Volume
- 30
- Category
- Article
- ISSN
- 0931-7597
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Zum Trocknen d a d die Verbindung nicht iiber 60Β° erhitzt werden. 3 -a -N a p h t h y l -p r o p a n o n -(3)-carbonsaure-(1) (VIII): Verb. V wird mit der dreifachen Menge 2nH,SO, 1 Stde. auf dem Waeserbade erhitzt. Die Ketosiiure scheidet sich dabei ale 01 auf der Oberflache ab. Nach dem Extrahiere
trans-1,3-Dihydroxy-1,3-dimethyl-1,3-disilacyclobutane. -With a view to getting more information about the conformation of dihydroxycyclocarbosilanes the title compound (II) is synthesized. The structure of (II) is determined by X-ray analysis. -(LYSSENKO, K. A.