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ChemInform Abstract: The Trigonal Prismatic Cluster Compound W6CCl15 and a Carambolage of Tungsten Clusters in the Structure of the Heteroleptic Cluster Compound W30C2(Cl,Br)68.

✍ Scribed by Markus Stroebele; H.-Juergen Meyer

Publisher: John Wiley and Sons
Year: 2010
Weight: 23 KB
Volume: 41
Category: Article
ISSN: 0931-7597
DOI: 10.1002/chin.201036014

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K 2 W 6 Br 14 (I), Rb 2 W 6 Br 14 (II), and Cs 2 W 6 Br 14 (III) were formed by reactions of W 6 Br 12 with the corresponding alkali metal bromides in evacuated silica tubes with a temperature gradient of 925 K/915 K. (I) crystallizes in the cubic space group Pn3 (no. 201), a = 13.808 A Ê , Z = 4, c