The Preparation of Stable α-Chlorosulfen
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Kristian Norup Koch; Grzegorz Mloston; Alexander Senning
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Article
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1999
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John Wiley and Sons
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English
⚖ 100 KB
The sterically crowded 2,2,4,4-tetramethyl-3-thioxocyclo-as the α-chlorosulfenyl chlorides 8 and 12 which yielded corresponding disulfides after treatment with equimolar butanone (7) and its dithio analogue 9 were found to react readily with gaseous chlorine to afford 1:1 and 1:2 adducts, amounts of