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ChemInform Abstract: Tetracyclic Alkaloids of the Sparteine Group. 1H and 13C NMR Spectroscopy and Conformational Analysis.

✍ Scribed by H. DUDDECK; J. SKOLIK; U. MAJCHRZAK-KUCZYNSKA

Book ID
112030003
Publisher
John Wiley and Sons
Year
2010
Weight
25 KB
Volume
27
Category
Article
ISSN
0931-7597

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Assignment of the 1H and 13C NMR spectra
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## Abstract The ^1^H and ^13^C NMR spectra of the pyrrolizidine alkaloid 13‐__O__‐acetyldicrotaline were studied at 4.7 T. A full assignment of the ^1^H and ^13^C signals was achieved by application of a variety of NMR techniques, including homonuclear ^1^H NOE difference, 2D Ξ΄~H~/Ξ΄~H~ phase‐sensit