ChemInform Abstract: Synthesis of α,β-Dibromo-β-nitrostyrene.
✍ Scribed by S. V. MAKARENKO; E. V. TRUKHIN; V. M. BERESTOVITSKAYA
- Publisher
- John Wiley and Sons
- Year
- 2010
- Weight
- 32 KB
- Volume
- 29
- Category
- Article
- ISSN
- 0931-7597
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The title compound is obtained by reacting u-cyano-4-nitrostyrene-p-ol with dicyclohexylcarbodiimide (molar ratio 21) at room temperature in tetrahydrofuran solvent. Esters of a-cyano-4-nitrostyrene-p-ol (1; HOCs(p-NO2)) are powerful acylating agents (1, 2). In the initial stage of our work in this