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ChemInform Abstract: Synthesis of the α-Tocopheramine-15N Model Compound 2,2,5,7,8-Pentamethyl-6-chromanylamine-15N.

✍ Scribed by Stefan Boehmdorfer; Lars Gille; Thomas Rosenau

Publisher: John Wiley and Sons
Year: 2010
Weight: 24 KB
Volume: 41
Category: Article
ISSN: 0931-7597
DOI: 10.1002/chin.201040137

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Total Synthesis of 15(RS)-5,6-Dehydro-8-epi-PGF2α Methyl Ester by a Biomimetic Process. -Using diacetone D-glucose (I) as starting material the first total synthesis of the title compound (IV) is achieved. Key step is a final biomimetic 5-exo-radical cyclization of the highly functionalized precurs