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ChemInform Abstract: Synthesis of Novel Octahydro-1,5-imino-3-benzazocin-4,7,10-trione Derivatives Having a Methyl Group at the C-2 Position as ABC Ring Models of Saframycins.

✍ Scribed by N. SAITO; M. TANITSU; T. BETSUI; R. SUZUKI; A. KUBO


Publisher
John Wiley and Sons
Year
2010
Weight
40 KB
Volume
28
Category
Article
ISSN
0931-7597

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✦ Synopsis


Synthesis of Novel Octahydro-1,5-imino-3-benzazocin-4,7,10-trione Derivatives Having a Methyl Group at the C-2 Position as ABC Ring Models of Saframycins.

-Simple and efficient syntheses of (Z)-3-benzylidenepiperazinedione ( VII) in both racemic and optically active forms are described. Compound (VII) is shown to be a useful intermediate for the effective construction of novel octahydrobenzazocintrione derivatives having a methyl group at the C-2 position (cf. (XIII)-(XVI)). -(SAITO, N.;