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ChemInform Abstract: Synthesis of Ethyl (13E)-Trifluoromethylretinoate and Its Analogues by Palladium-Catalyzed Cross-Coupling.

✍ Scribed by Jerome Thibonnet; Gildas Prie; Mohamed Abarbri; Alain Duchene; Jean-Luc Parrain

Publisher: John Wiley and Sons
Year: 2010
Weight: 30 KB
Volume: 30
Category: Article
ISSN: 0931-7597
DOI: 10.1002/chin.199929177

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✦ Synopsis

Synthesis of Ethyl (13E)-Trifluoromethylretinoate and Its Analogues by Palladium-Catalyzed Cross-Coupling. -Stille coupling of the (Z)-vinyl iodide (I) with the bis(tributylstannyl)ethylene (II) affords the (E,E)ester (III) after iododestannylation. Compound (III) is a key intermediate for the synthesis of dienynes (V) or the title compound (VII). -(THIBONNET,

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