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ChemInform Abstract: Synthesis of Dimer Phosphoramidite Synthons for Oligodeoxyribonucleotide Phosphorothioates Using Diethyldithiocarbonate Disulfide as an Efficient Sulfurizing Reagent.

✍ Scribed by Alessandra Eleuteri; Zacharia S. Cheruvallath; Daniel C. Capaldi; Douglas L. Cole; Vasulinga T. Ravikumar


Publisher
John Wiley and Sons
Year
2010
Weight
29 KB
Volume
30
Category
Article
ISSN
0931-7597

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✦ Synopsis


Synthesis of Dimer Phosphoramidite Synthons for Oligodeoxyribonucleotide Phosphorothioates Using Diethyldithiocarbonate Disulfide as an Efficient Sulfurizing Reagent. -An efficient solution-phase synthesis of deoxyribonucleoside phosphorothioate dimers utilizing the phosphoramidite approach is described. Diethyldithiocarbonate disulfide (DDD) is found to be an efficient sulfurizing reagent in the conversion of phosphite triesters to phosphorothioate triesters. -(ELEUTERI, ALESSANDRA; CHERUVALLATH,