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ChemInform Abstract: Synthesis of Chiral Organotin Reagents: Diels—Alder Reactions of Methyl 3-(Triphenylstannyl)acrylate: Synthesis of Diphenyl-(3-Substituted Bicyclo[2.2.1]heptan-2-yl)tin Hydrides.

✍ Scribed by A. H. MCNEILL; S. V. MORTLOCK; R. M. PRATT; E. J. THOMAS

Publisher
John Wiley and Sons
Year
2010
Weight
38 KB
Volume
29
Category
Article
ISSN
0931-7597

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✦ Synopsis

Synthesis of Chiral Organotin

Reagents: Diels-Alder Reactions of Methyl 3-(Triphenylstannyl)acrylate: Synthesis of Diphenyl-(3-Substituted Bicyclo[2.2.1]heptan-2-yl)tin Hydrides.

-Synthetic routes to racemic, functionalized bicycloheptanyltin hydrides, e.g. (IX), (XII) ,and (XIII), are described. These compounds are found to undergo free-radical reactions as exemplified by addition to methyl propiolate (I) and reductive dehalogenation of iodo lactone (XVI). -(MCNEILL, A. H.; MORTLOCK,

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