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ChemInform Abstract: Synthesis of Benzoyl and Dodecanoyl Derivatives from Protected Carbohydrates under Focused Microwave Irradiation.

✍ Scribed by C. LIMOUSIN; J. CLEOPHAX; A. LOUPY; A. PETIT

Publisher
John Wiley and Sons
Year
2010
Weight
33 KB
Volume
30
Category
Article
ISSN
0931-7597

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✦ Synopsis

Synthesis of Benzoyl and Dodecanoyl Derivatives from Protected

Carbohydrates under Focused Microwave Irradiation.

-Carbohydrates with either one secondary, one primary, or two secondary hydroxyl groups are studied in the phase transfer catalyzed transesterification in basic medium with aromatic or fatty acid esters (II). Small amounts of DMF are necessary to provide good yields within 15 to 30 minutes. Specific activation by microwaves when compared to conventional heating in the same conditions is largely evidenced and is more important when the dodecanoyl group is involved.

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