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ChemInform Abstract: Synthesis of Aryl Phosphonates by Reaction of Grignard Reagents with Diethyl Cyanophosphonate.

✍ Scribed by Angel Guzman; Ricardo Alfaro; Eduardo Diaz

Publisher
John Wiley and Sons
Year
2010
Weight
27 KB
Volume
30
Category
Article
ISSN
0931-7597

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## Abstract Diethyl (1‐cyanoethyl) phosphorate 1 was reacted with __n__‐butyl‐lithium in tetrahydrofuran (THF) at ‐ 78 Β°C and the resulting carbanion 2 reacted with perfluoroalkanoic add anhydride to afford perfluoroacylated phosphorate 3. Without isolation 3 was attacked by Grignard reagents givin

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## Abstract ChemInform is a weekly Abstracting Service, delivering concise information at a glance that was extracted from about 100 leading journals. To access a ChemInform Abstract of an article which was published elsewhere, please select a β€œFull Text” option. The original article is trackable v