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ChemInform Abstract: Synthesis of 3-Hydroxy-2-hydroxy(phenyl)methyl-3-methyl-2,3-dihydro-4H-furo [3,2-c]chromen-4-one from 4-Hydroxycoumarin.

✍ Scribed by I. A. Os'kina; Yu. V. Gatilov; A. Ya. Tikhonov

Book ID: 112043731
Publisher: John Wiley and Sons
Year: 2012
Weight: 21 KB
Volume: 43
Category: Article
ISSN: 0931-7597
DOI: 10.1002/chin.201218154

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4-Oxo-3,4-dihydro-2-chromen-3-yl acetate is synthesized using manganese(III)acetate starting from 2,3-dihydro-4Hchromen-4-one. K 2 CO 3 mediated hydrolysis of 4-oxo-3,4-dihdro-2-chromen-3-yl acetate furnished 3-hydroxy-2,3-dihydro-4Hchromen-4-one in high yield.The enantioselective hydrolysis of (±)-