ChemInform Abstract: Synthesis and Structural Studies of 5,11,17,23-Tetrahydroxyresorc[4]arenes.
✍ Scribed by Thorsten Gerkensmeier; Ceno Agena; Waldemar Iwanek; Roland Froehlich; Sirpa Kotila; Christian Naether; Jochen Mattay
- Publisher
- John Wiley and Sons
- Year
- 2010
- Weight
- 25 KB
- Volume
- 33
- Category
- Article
- ISSN
- 0931-7597
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📜 SIMILAR VOLUMES
We report herein the observation of a hexameric structure of only by hydrogen bonds. The tendency to form aggregates in solution is demonstrated mainly by means of ESI-MS a hydroxyresorc [4]arene in the solid state, enclosing a large interior space. This artificial molecular container is stabilized
## Abstract Treatment of 5,11,17,23‐tetrakis[(__p__‐carboxyphenyl)azo]‐25,26,27,28‐tetrahydroxy calix[4]arene (**2**) with HCl in DMF or NaOH in MeOH produced 5,11,17,23‐tetrakis[(__p__‐carboxyphenyl)azo]‐25,26,27,28‐tetrahydroxycalix[4]‐arene·4DMF (2·4DMF) and 5,11,17,23‐tetrakis[(__p__‐carboxyphe