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ChemInform Abstract: Synthesis and Crystal Structure of the Borate-Phosphate: α-Zn3( BO3)(PO4).

✍ Scribed by K. BLUHM; C. H. PARK

Publisher
John Wiley and Sons
Year
2010
Weight
32 KB
Volume
28
Category
Article
ISSN
0931-7597

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✦ Synopsis

1997 structure structure (solids and liquids) D 2000

19 -015

Synthesis and Crystal Structure of the Borate-Phosphate: α-Zn3( BO3)(PO4).

-Single crystals of the title compound are prepared by reacting B2O3, P2O5, and Zn(OH)2•ZnCO3 at 1050 • C (Pt-crucible, air, 6 h) . The compound crystallizes in the monoclinic space group Cm with Z = 4. Zn is present in trigonal-bipyramidal, tetragonal-pyramidal, and distorted tetrahedral oxygen coordination. The boron atoms are present in isolated planar BO3 units and the P atoms form PO4 tetrahedra which are linked by the ZnO5 bipyramids. -(BLUHM, K.;

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