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ChemInform Abstract: Synthesis and Crystal Structure of Metal(I) Hydrogen Sulfates — Ag(H3O)(HSO4)2, Ag2(HSO4)2(H2SO4), AgHSO4, and Hg2(HSO4)2.

✍ Scribed by A. Stiewe; E. Kemnitz; S. Troyanov

Publisher
John Wiley and Sons
Year
2010
Weight
29 KB
Volume
30
Category
Article
ISSN
0931-7597

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✦ Synopsis

Synthesis and Crystal Structure of Metal(I) Hydrogen Sulfates -Ag(H 3 O)(HSO 4 ) 2 , Ag 2 (HSO 4 ) 2 (H 2 SO 4 ), AgHSO 4 , and Hg 2 (HSO 4 ) 2 .

-The silver hydrogen sulfates of title are synthesized from Ag 2 SO 4 in hot conc. H 2 SO 4 . Hg 2 (HSO 4 ) 2 is obtained from metallic Hg in conc. H 2 SO 4 . The structures of all compounds are determined by single crystal XRD and the metal coordinations and hydrogen bonding schemes are described. Ag(H 3 O)(HSO 4 ) 2 and Hg 2 (HSO 4 ) 2 crystallize in the monoclinic space group P2 1 /c with Z = 4, AgHSO 4 also belongs to space group P2 1 /c, Z = 16, and Ag 2 (HSO 4 ) 2 (H 2 SO 4 ) is orthorhombic (space group Pna2 1 , Z = 4). -(STIEWE, A.; KEMNITZ,

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