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ChemInform Abstract: Synthesis and Crystal Structure of a Barium Zinc Vanadyl Phosphate, BaZn(VO)(PO4)2, Containing ((VO)PO4) Layers.

✍ Scribed by S. MEYER; HK. MUELLER-BUSCHBAUM

Publisher: John Wiley and Sons
Year: 2010
Weight: 30 KB
Volume: 28
Category: Article
ISSN: 0931-7597
DOI: 10.1002/chin.199728006

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✦ Synopsis

Synthesis and Crystal Structure of a Barium Zinc Vanadyl Phosphate, BaZn(VO)(PO4)2, Containing ((VO)PO4) Layers.

-Single crystals of the title compound are prepared by solid state reaction of a prereacted mixture of BaCO3 and P2O5 (800 • C, 24 h, air) with ZnO, V2O3, and V2O5 (780 • C, 72 h, evacuated quartz tube). BaZn(VO)(PO4)2 crystallizes in the orthorhombic space group Pbca with Z = 8 (single crystal XRD). The structure is characterized by layers of PO4 tetrahedra and square VO1+5 pyramids connected by layers of PO4 and ZnO4 tetraheda. The resulting tunnel structure is filled by the Ba2+ ions.

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