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ChemInform Abstract: Synthesis and Conformational Studies of Pentahydroxy(2.1.2.1.1)- and Hexahydroxy(2.1.1.1.1.1)metacyclophanes.

✍ Scribed by T. YAMATO; M. YASUMATSU; L. K. DOAMEKPOR; S. NAGAYAMA

Book ID
112022365
Publisher
John Wiley and Sons
Year
2010
Weight
25 KB
Volume
26
Category
Article
ISSN
0931-7597

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Synthesis and conformational studies of
Synthesis and conformational studies of pentahydroxy[2.1.2.1.1]- and hexahydroxy [2.1.1.1.1.1]metacyclophanes
✍ Yamato, Takehiko ;Yasumatsu, Masashi ;Doamekpor, Louis Korbla ;Nagayama, Souichi 📂 Article 📅 1995 🏛 John Wiley and Sons 🌐 English ⚖ 457 KB

## Abstract Base‐catalyzed condensation of 1,2‐bis[5‐__tert__‐butyl‐3‐(5‐__tert__‐butylsalicyl)‐2‐hydroxyphenyl]ethane (8) with formaldehyde in xylene affords a novel ethylene‐bridged calixarene‐analogous macrocyclic metacyclophane. However, not the desired 2 has been obtained. Instead, the novel m