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ChemInform Abstract: Synthesis and Characterization of the First Examples of 1,3,2-Diazastibole and 1,3,2-Diazabismole Ring Compounds.

✍ Scribed by Bruce N. Diel; Timothy L. Hubler; Wiliam G. Ambacher

Publisher
John Wiley and Sons
Year
2010
Weight
32 KB
Volume
30
Category
Article
ISSN
0931-7597

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✦ Synopsis

Abstract

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Synthesis and characterization of the fi
Synthesis and characterization of the first examples of 1,3,2-diazastibole and 1,3,2-diazabismole ring compounds
✍ Bruce N. Diel; Timothy L. Huber; William G. Ambacher πŸ“‚ Article πŸ“… 1999 πŸ› John Wiley and Sons 🌐 English βš– 229 KB

Reaction of either 9, or diphenylethanedione (benzil) with two equivalents of Li[N(SiMe 3 ) 2 ], followed by quenching of the reaction with excess Cl-SiMe 3 , produces the corresponding N,NЈbis(trimethylsilyl)-␣-diimines in high yields (85-95%). Subsequent dehalosilylation/ring-closure reactions wi