✍ Scribed by T. M. KRUELLE; C. DE LA FUENTE; K. A. WATSON; M. GREGORIOU; L. N. JOHNSON; K. E. TSITSANOU; S. E. ZOGRAPHOS; N. G. OIKONOMAKOS; G. W. J. FLEET
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Stereospecific Synthesis of Spirohydantoins of β-Glucopyranose: Inhibitors of Glycogen Phosphorylase.
-The key intermediate in the synthesis of title compounds (VIII), the bicyclic lactone (V), is readily prepared from azidolactone (I) (or its α-azido isomer). The rigid structure of (V) guarantees the . beta.-configuration of the nitrogen function after ring opening of the lactone by attack of ammonia, amines, hydrazine, or hydroxylamine. -(KRUELLE, T. M.;
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