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ChemInform Abstract: Stereoselective Transformation of Enantiopure Cyclohexenol into cis- Hydrindan. An Enantioselective Formal Total Synthetic Route to (+)- Pumiliotoxin C.

✍ Scribed by M. TOYOTA; T. ASOH; M. MATSUURA; K. FUKUMOTO


Publisher
John Wiley and Sons
Year
2010
Weight
32 KB
Volume
28
Category
Article
ISSN
0931-7597

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✦ Synopsis


Stereoselective Transformation of Enantiopure Cyclohexenol into cis-Hydrindan. An Enantioselective Formal Total Synthetic Route to (+)-Pumiliotoxin C. -Starting from the known chiral acid (I) the biologically interesting title compound (IX) is synthesized. Key step in this approach is the cyclization to the cis-hydrindan (VI) under mild conditions without the high dilution technique and the long reaction time required in the radical step. -(TOYOTA, M.;