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ChemInform Abstract: Stereoselective Synthesis of (R)- and (S)-2-Methyl-3-oxo-3,4-dihydro-2H-1,4-benzoxazine-2-carboxylic Acids, -carboxylates and -carboxamides.

✍ Scribed by Matej Breznik; Valentina Hrast; Alenka Mrcina; Danijel Kikelj

Publisher: John Wiley and Sons
Year: 2010
Weight: 33 KB
Volume: 30
Category: Article
ISSN: 0931-7597
DOI: 10.1002/chin.199928190

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## Abstract For Abstract see ChemInform Abstract in Full Text.

Enantiomers of 2-methyl- and 2,4-dimethy

Enantiomers of 2-methyl- and 2,4-dimethyl-3-oxo-3,4-dihydro-2H-1,4-benzoxazine-2-carboxylic acid: Preparation by resolution, determination of absolute configuration, and Curtius rearrangement

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Both enantiomers of 2-methyl-3-oxo-3,4-dihydro-2H-1,4-benzoxazine-2carboxylic acid 2 and 2,4-dimethyl-3-oxo-3,4-dihydro-2H-1,4-benzoxazine-2-carboxylic acid 3 were prepared via resolution of the corresponding racemic carboxylic acids with (R)-and (S)-1-phenylethylamine, respectively. Absolute config